Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. has developed the application of Shimadzu capillary chromatography column for industrial analysis of chlorinated n-butane. The HH-1701 capillary column gas chromatography method is used to determine the organic content in chlorinated n-butane by-products. The sample is subjected to pre-treatment, , FID is used for detection, and area normalization is used for quantification. Good linear relationship, R2 greater than 0.997, detection limit between 2.8~8.9 μ g/mL, relative standard deviation (RSD) of method repeatability between 2.9%~9.8%, and sample recovery rate between 92.7%~110.5%. The method is simple, with good precision and accuracy, and can meet the detection requirements.
本标准规定了工业用氯代正丁烷的要求、试验方法、检验规则和标志、包装、运输和贮存。
本标准适用于由正丁醇和盐酸为原料反应生产的氯代正丁烷。
名称：毛细管柱
固定液： 7%-氰丙基 - 7%苯基-86%甲基聚硅氧烷
规格：30m*0.32mm*0.5um
型号：HH-1701
应用：HG_T 5381-2018 工业用氯代正丁烷
适用于：
安捷伦490在线/便携，4890,5890,6890,7820,7890,8860,8890
岛津GC-14C，GC-2010，GC-2014，GC-2030
赛默飞1310,1300,1610,1600
瓦里安3800系列
布鲁克PE580,590,680,690
磐诺A90，福立GC9790，华爱，天瑞，天美，GC7900，川仪，北分瑞利，东西电子，鲁南瑞虹，捷岛/科晓
浩瀚色谱(山东)应用技术开发有限公司，研制《工业用氯代正丁烷分析毛细色谱柱应用岛津》采用HH-1701毛细管柱气相色谱法测定氯代正丁烷副产物中的有机物含量,试样经过前处理,,FID为检测,面积归一进行定量。良好的线性关系,R2大于0.997,检出限在2.8~8.9μg/mL之间,方法重复性相对标准偏差(RSD)在2.9%~9.8%之间,试样加标回收率在92.7%~110.5%之间。方法简单,具有较好的精密度和准确度,能满足检测要求。
滕州市浩瀚色谱仪器技术服务有限公司
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