GB/T 43571-2023
本文件描述了玩具材料中11种可迁移有机锡测定的气相色谱-串联质谱法.本文件适用于玩具材料中甲基锡(MeT),二甲基锡(DMT),二丙基锡(DProT),丁基锡(BuT),二丁基锡(DBT),三丁基锡(TBT),正辛基锡(MOT),二辛基锡(DOT),四丁基锡(TeBT),二苯基锡(DPhT),三苯基锡(TPhT)11种可迁移有机锡的测定.
名称：安捷伦GC8860玻璃柱
规格：6ft*1/4
型号：10%DC550/Chromosorb WAW DMCS 60-80目
zui高使用温度：240°C
应用：单丁基三氯化锡，二丁基二氯化锡
浩瀚色谱（山东）应用技术开发有限公司，研制生产的《DC-550玻璃色谱柱应用安捷伦8890TCD》，提出了以乙基溴化镁作为衍生化试剂 ,将二丁基二氯化锡转化成低沸点、易汽化的二丁基二乙基锡 ,采用四丁基锡作内标 ,测定二丁基二氯化锡含量的气相色谱法。方法具有分析速度快、准确度高、重现性好等优点。此方法回收率为 97.5 % -1 0 0.9% 。
适用于：
安捷伦490在线/便携，4890,5890,6890,7820,7890,8860,8890
岛津GC-14C，GC-2010，GC-2014，GC-2030
赛默飞1310,1300,1610,1600
瓦里安3800系列
布鲁克PE580,590,680,690
磐诺A90，福立GC9790，华爱，天瑞，天美，GC7900，川仪，北分瑞利，东西电子，鲁南瑞虹，捷岛/科晓
GB/T 43571-2023
This document describes the gas chromatography tandem mass spectrometry method for the determination of 11 transferable organotin compounds in toy materials This document is applicable for the determination of 11 migratory organotin compounds in toy materials, including methyl tin (MeT), dimethyl tin (DMT), dipropyltin (DProT), butyl tin (BuT), dibutyltin (DBT), tributyltin (TBT), octyltin (MOT), dioctyltin (DOT), tetrabutyltin (TeBT), diphenyltin (DPhT), and triphenyltin (TPhT)
Name: Agilent GC8860 Glass Column
Specification: 6ft * 1/4
Model: 10% DC550/Chromosorb WAW DMCS 60-80 mesh
Maximum operating temperature: 240 ° C
Application: Monobutyl tin trichloride, dibutyl tin dichloride
Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. has developed and produced the "DC-550 Glass Chromatography Column Application Agilent 8890TCD", which proposes using ethyl magnesium bromide as a derivatization reagent to convert dibutyltin dichloride into low boiling point, easily vaporized dibutyltin, and using tetrabutyltin as an internal standard to determine the content of dibutyltin dichloride by gas chromatography. The method has the advantages of fast analysis speed, high accuracy, and good reproducibility. The recovery rate of this method is 97.5% -100.9%.
Suitable for:
Agilent 490 online/portable, 48905890689088608890
Shimadzu GC-14C, GC-2010, GC-2014, GC-2030
Thermo Fisher Scientific 1310130016101600
Varian 3800 Series
Brooke PE580590680690
Panno A90, Fuli GC9790, Huaai, Tianrui, Tianmei, GC7900， Chuanyi, Beifen Ruili, Dongxi Electronics, Lunan Ruihong, Jiedao/Kexiao
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